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Journal of Systems Chemistry
Scheme 7 | Journal of Systems Chemistry

Scheme 7

From: Design and synthesis of nucleolipids as possible activated precursors for oligomer formation via intramolecular catalysis: stability study and supramolecular organization

Scheme 7

Synthesis of the ribose and deoxyribose nucleolipids. a) 12,1H-tetrazole, dry DCM, rt 4 h; b) 13, 1H-tetrazole, dry DCM, rt 4 h; c) H2O2, -78°C - rt, 30 min; d) H2, Pd/C, THF, K2CO3, H2O, rt 48 h, for 32 and 41, MeOH was used as co-solvent without adding K2CO3. 30, 36, 39 and 45 were isolated as 2 K+ salt.

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